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WebCorresponding pore-size distributions can be found in Figures S18 and S19. TGA traces of empty and loaded samples of (e) MOF-808 and (f) MOF-808_act. Corresponding analyses of first derivatives ... WebJul 13, 2024 · Analyzes were carried out using a Simultaneous TGA-DTA thermal-analyzer type SDT 2960 Simultaneous TGA-DTA from TA Instruments, Champaign, IL, USA) at temperatures ranging from 20 °C to 1000 °C, at a heating rate of 10 °C·min −1, under atmospheric air with samples of ca. 2–4 mg. WebMar 3, 2024 · TGA verified the lack of solvent molecules in the pores while the PXRD pattern matched that of the parent MOF, PCN-57 (Fig. 3c and S19 †). To confirm the presence of the MIM linker in the MOF, a sample was digested in K 3 PO 4 /D 2 O/d 6-DMSO and the ratio of 3 to TTDC of 1 : 8 calculated from the solution 1 H NMR spectrum (Fig. S16 ... hayes morris house butte